Table 3
Main similarities and differences between the three standards ASTM 2765-16, IEC FDIS 62788 and GB/T29848-2018.
Equipment | |
ASTM 2765-16 | Round-bottom flask, reflux condenser |
GB/T29848-2018 | Reaction flask, reflux condenser |
IEC FDIS 62788 | Soxhlet apparatus or similar |
Solvent | |
ASTM 2765-16 | Xylene or decahydronaphtalene |
GB/T29848-2018 | Xylene |
IEC FDIS 62788 | Xylene, toluene or tetrahydrofuran (THF) |
Particle size | |
ASTM 2765-16 | Grinded particles which pass through 30-, but not through 60- mesh |
GB/T29848-2018 | < (3 × 3) mm2 |
IEC FDIS 62788 | Small pieces (size not mentioned) |
Antioxidant | |
ASTM 2765-16 | 1%, e.g. 2,2′-methylenebis(4-methyl-6-tert-butylphenol) |
GB/T29848-2018 | Not specified |
IEC FDIS 62788 | 2% wt. of the EVA, e.g. 2,2′-methylenebis(4-methyl-6-tert-butylphenol) or 2,6 di-tert-butyl-4-methylphenol (BHT) |
Extraction duration | |
ASTM 2765-16 | 12 h (xylene) |
GB/T29848-2018 | 5 h |
IEC FDIS 62788 | ≥ 8 h (for xylene), for expected GC < 70% ≥ 12 h; ≥ 15 cycles per hour for other solvents time has to be adapted. |
Placement of sample | |
ASTM 2765-16 | Into hot solvent |
GB/T29848-2018 | Into cold solvent, heating up |
IEC FDIS 62788 | Not specified |
Replacement of sample | |
ASTM 2765-16 | Not specified |
GB/T29848-2018 | Not specified |
IEC FDIS 62788 | Not specified |
Drying | |
ASTM 2765-16 | 150 °C, to constant weight |
GB/T29848-2018 | 140 °C, to constant weight |
IEC FDIS 62788 | 115 °C, to constant weight, ≥4 h |
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